HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Difluoroaniline → HCID 178512264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Difluoroaniline | HCID 77469 | — |
| Reactant | Diphenyl N-Cyanocarbonimidate | HCID 688090 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 178512264 | HCID 178512264 | 86.4% |
Reaction Steps
To a solution of 3,4-difluoroaniline (646 mg, 5 mmol) in isopropanol (10 mL) was added diphenyl cyanocarbonimidate (1.19 g, 5 mmol) and the suspension was stirred at room temperature over night. The precipitate was filtered off, washed with isopropanol and dried under reduced pressure to yield the title compound as a white solid (1.18 g, 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486967B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-9229aa3c4d2446089f67ca26b6ef5c2b |
| Source note | uspto-grants-2013_07 |