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HRID451770

反应详情

EQUATION

反应方程式

HRID 451770 的结构方程式

REACTANTS

反应物

2
结构：CN
HCID6329

Methylamine

CH5N

结构：CCC(OS(=O)(=O)c1ccc(C)cc1)[C@H](CC1CCCCC1)NC(=O)OC(C)(C)C
HCID59201516

未命名化合物

PRODUCTS

生成物

1
结构：CCC(NC)[C@H](CC1CCCCC1)NC(=O)OC(C)(C)C
HCID59201714

未命名化合物

PROCEDURE

实验过程

A solution of (S)-2-(tert-butoxycarbonylamino)-1-cyclohexylpentan-3-yl 4-methylbenzenesulfonate (640 mg, 1.46 mmol) in 33% MeNH2 (in EtOH) (0.02 M) was heated to 60° C. for 1 h in a pressure sealed vessel. The solvent was removed under reduced pressure to give (S)-tert-butyl 1-cyclohexyl-3-(methylamino)pentan-2-ylcarbamate. MS ESI +ve m/z 299 (M+H).

WORKUP

后处理

  1. customsealed vessel
  2. customThe solvent was removed under reduced pressure