HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Fluoro-2-methoxy-4-nitrobenzene → HCID 59536597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Fluoro-2-methoxy-4-nitrobenzene | HCID 14451968 | — |
| Reactant | 3-({[tert-Butyl(diphenyl)silyl]oxy}methyl)pyridin-2(1H)-one | HCID 59410156 | — |
| Product | HCID 59536597 | HCID 59536597 | — |
Reaction Steps
Analogously to Example 4A, 5.00 g (13.8 mmol) of the compound from Example 3A are reacted with 2.59 g (15.1 mmol) of 1-fluoro-2-methoxy-4-nitrobenzene. The product is purified by chromatography on silica gel (mobile phase pentane/ethyl acetate=5:1), giving 2.70 g (38% of theory) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08487111B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-ef255e550a4641abb9ea742051007ba2 |
| Source note | uspto-grants-2013_07 |