Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66886440 | — |
| Solvent | 2,2,4-Trimethylpentane | HCID 10907 | — |
| Product | HCID 44481633 | HCID 44481633 | — |
Reaction Steps
A mixture of 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine (30 mg, 0.10 mmol), n-butan-1-amine (0.50 ml, 5.1 mmol) and EtOH (1.0 ml) was heated under microwave radiation at 130° C. for 30 min. MS m/z (rel. intensity, 70 eV) 299 (M+, 1), 123 (8), 86 (bp), 77 (9), 72 (10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08492372B2 |
|---|
| Source dataset | uspto-grants-2013_07 |
|---|
| ORD ID | ord-fcc7d9369ac84858930d38916068ad7d |
|---|
| Source note | uspto-grants-2013_07 |
|---|
