HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 44481898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66886440 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44481898 | HCID 44481898 | — |
Reaction Steps
Preparation according to Example 22 using 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine (30 mg, 0.10 mmol), prop-2-en-1-amine (0.50 ml, 6.7 mmol) and EtOH (1.0 ml). MS m/z (rel. intensity, 70 eV) 283 (M+, 1), 123 (6), 77 (7), 71 (5), 70 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492372B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-d13403493b2647ce8b3e31c41008ad7f |
| Source note | uspto-grants-2013_07 |