HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylethylamine → HCID 44482174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylethylamine | HCID 12219 | — |
| Reactant | 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66886440 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44482174 | HCID 44482174 | — |
Reaction Steps
Preparation according to Example 22 using 2-(bromomethyl)-7-(methylsulfonyl)-4H-1,3-benzodioxine (30 mg, 0.10 mmol), N-methylethanamine (0.50 ml, 5.8 mmol) and EtOH (1.0 ml). MS m/z (rel. intensity, 70 eV) 285 (M+, 1), 77 (4), 73 (5), 72 (bp), 51 (3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492372B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-a39f932767fd4d50aa1b4ea48f87edd2 |
| Source note | uspto-grants-2013_07 |