HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanamine, N-ethyl- → HCID 44482449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanamine, N-ethyl- | HCID 88398 | — |
| Reactant | 2-(bromomethyl)-5-fluoro-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66887621 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44482449 | HCID 44482449 | — |
Reaction Steps
Preparation according to Example 34 using 2-(bromomethyl)-5-fluoro-7-(methylsulfonyl)-4H-1,3-benzodioxine (8.5 mg, 0.026 mmol), N-ethylpropan-1-amine (0.5 ml) and EtOH (3 ml). MS m/z (rel. intensity, 70 eV) 331 (M+, 0.1), 101 (7), 100 (bp), 95 (5), 72 (14), 58 (12).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492372B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-6b19c0cd5de74c31bfe2219b3882a924 |
| Source note | uspto-grants-2013_07 |