HuagongsheHuagongshe Chemistry Print Report · For research reference only
Neopentylamine → HCID 44478534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Neopentylamine | HCID 79882 | — |
| Reactant | 2-(bromomethyl)-5-fluoro-7-(methylsulfonyl)-4H-1,3-benzodioxine | HCID 66887621 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44478534 | HCID 44478534 | — |
Reaction Steps
Preparation according to Example 34 using 2-(bromomethyl)-5-fluoro-7-(methylsulfonyl)-4H-1,3-benzodioxine (8.5 mg, 0.026 mmol), 2,2-dimethylpropan-1-amine (0.5 ml) and EtOH (3 ml). MS m/z (rel. intensity, 70 eV) 331 (M+, 1), 274 (74), 203 (20), 141 (32), 100 (bp), 72 (74).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492372B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-322021c146e14c84ae75d4b56d8a63c9 |
| Source note | uspto-grants-2013_07 |