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HRID45247

反应详情

EQUATION

反应方程式

HRID 45247 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)C(C=O)C(C(=O)OCC)c1ccccc1
HCID13486182

未命名化合物

结构：CC(C)(C)NS(=O)(=O)c1ccc(NN)nc1
HCID16777776

未命名化合物

结构：COC(=O)C(c1ccccc1)c1c[nH]n(-c2ccc(S(=O)(=O)NC(C)(C)C)cn2)c1=O
HCID86659744

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)C(c1ccccc1)c1c[nH]n(-c2ccc(S(=O)(=O)NC(C)(C)C)cn2)c1=O
HCID86659743

未命名化合物

PROCEDURE

实验过程

According to the process described in Example 27.2, starting with 2 g (7.19 mmol) of diethyl 2-formyl-3-phenylbutanedioate and 1.75 g (7.19 mmol) of N-tert-butyl-6-hydrazinylpyridine-3-sulfonamide, 3.1 g of methyl {2-[5-(tert-butylsulfamoyl)pyridin-2-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}(phenyl)acetate are obtained in the form of a powder.

WORKUP

后处理

  1. customare obtained in the form of a powder