HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13486182, compound → ethyl {2-[5-(tert-butylsulfamoyl)pyridin-2-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-(phenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13486182 | HCID 13486182 | — |
| Reactant | HCID 16777776 | HCID 16777776 | — |
| Reactant | methyl {2-[5-(tert-butylsulfamoyl)pyridin-2-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}(phenyl)acetate | HCID 86659744 | — |
| Product | ethyl {2-[5-(tert-butylsulfamoyl)pyridin-2-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-(phenyl)acetate | HCID 86659743 | — |
Reaction Steps
According to the process described in Example 27.2, starting with 2 g (7.19 mmol) of diethyl 2-formyl-3-phenylbutanedioate and 1.75 g (7.19 mmol) of N-tert-butyl-6-hydrazinylpyridine-3-sulfonamide, 3.1 g of methyl {2-[5-(tert-butylsulfamoyl)pyridin-2-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}(phenyl)acetate are obtained in the form of a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541455B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-f8fe0cac2ea2482cb3c026f5c50bb6c8 |
| Source note | uspto-grants-2013_09 |