HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 17984208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 69036029 | HCID 69036029 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 17984208 | HCID 17984208 | — |
Reaction Steps
3-(4-phenylimidazol-1-yl)propionic acid ethyl ester (2.442 g, 10 mmol) was dissolved in 50 mL of ethanol, added with 0.5N-NaOH (20 mL) and then stirred at room temperature. Initiation and termination of the reaction was confirmed with TLC (EtOAc). Upon completion of the reaction, ethanol was removed by distillation under reduced pressure to obtain the target compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492384B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-0d9fcb685f3b451dba5ef9964c64dcf3 |
| Source note | uspto-grants-2013_07 |