HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetoxyisobutyroyl chloride → HCID 68663477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetoxyisobutyroyl chloride | HCID 123496 | — |
| Reactant | HCID 68664363 | HCID 68664363 | — |
| Product | HCID 68663477 | HCID 68663477 | 66% |
Reaction Steps
In the same manner as in Reference Example 129 and using 1-[4-(trifluoromethoxy)phenyl]-1H-benzimidazole-6-carbohydrazide instead of 3-bromo-1-benzofuran-5-carbohydrazide and 2-chloro-1,1-dimethyl-2-oxoethyl acetate instead of (1S)-2-chloro-1-methyl-2-oxoethyl acetate, the title compound (yield 66%) was obtained as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492378B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-ccb68aba67a0408495b156d959e58a15 |
| Source note | uspto-grants-2013_07 |