HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 68663951, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 68663978 | HCID 68663978 | — |
| Product | HCID 68663951 | HCID 68663951 | 84% |
Reaction Steps
In the same manner as in Example 140 and using 5-[3-[3-chloro-4-(methylsulfinyl)phenyl]-1-benzofuran-5-yl]-1,3,4-oxadiazol-2-amine instead of 2-methyl-5-[3-[4-(methylthio)phenyl]-1-benzofuran-5-yl]-1,3,4-oxadiazole and using N,N-dimethylformamide instead of dichloromethane, the title compound (yield 84%) was obtained as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492378B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-2b18ccceb5d54da1800fd1601deb7359 |
| Source note | uspto-grants-2013_07 |