HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine tetrahydrofuran → HCID 68663400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine tetrahydrofuran | HCID 66615946 | — |
| Reactant | HCID 68663200 | HCID 68663200 | — |
| Product | HCID 68663400 | HCID 68663400 | 65% |
Reaction Steps
In the same manner as in Example 110 and using 2-[3-(2-chlorophenyl)-1-benzofuran-5-yl]-5-(methylsulfonyl)-1,3,4-oxadiazole instead of 2-(2,3-dihydro-1-benzofuran-5-yl)-5-(methylsulfonyl)-1,3,4-oxadiazole and using 2M methylamine-tetrahydrofuran solution instead of 3-fluorobenzylalcohol, the title compound (yield 65%) was obtained as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492378B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-deee75910ed343c09678b2af81664805 |
| Source note | uspto-grants-2013_07 |