HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 68663868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-(Methylsulfonyl)-5-[3-[4-(trifluoromethoxy)phenyl]-1-benzofuran-5-yl]-1,3,4-oxadiazole | HCID 68664360 | — |
| Product | HCID 68663868 | HCID 68663868 | 4% |
Reaction Steps
In the same manner as in Example 110 and using 2-(methylsulfonyl)-5-[3-[4-(trifluoromethoxy)phenyl]-1-benzofuran-5-yl]-1,3,4-oxadiazole instead of 2-(2,3-dihydro-1-benzofuran-5-yl)-5-(methylsulfonyl)-1,3,4-oxadiazole and using methanol instead of 3-fluorobenzyl alcohol, the title compound (yield 4%) was obtained as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492378B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-af37050f2955438d8bb8af30b635f033 |
| Source note | uspto-grants-2013_07 |