HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 131730725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 3-Quinuclidinol, (-)- | HCID 91404 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131730725 | HCID 131730725 | — |
Reaction Steps
The reaction of (R)-3-Quinuclidinol with carbonyldiimidazole (CDI) in dichloromethane, at 0° C. during 4 h, afford the corresponding imidazolide carbamate (intermediate 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492402B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-7638632b5d60435fa57e99388de317c4 |
| Source note | uspto-grants-2013_07 |