Trifluoroacetic acid → HCID 58508464, compound

Participants

Reaction Steps

Thioanisole (2.3 mL) and trifluoroacetic acid (7.7 mL) were added to the obtained tert-butyl 2-(2-(benzyloxy)-5-(oxazol-5-yl)benzamido)-4-phenylbenzoate (0.21 g), followed by stirring at room temperature for 9 hours and 40 minutes. The solvent was evaporated under reduced pressure, and methanol was added to the residue. The solid substance was collected by filtration to obtain 0.12 g of 2-(2-hydroxy-5-(oxazol-5-yl)benzamido)-4-phenylbenzoic acid as a white solid.

Provenance & Evidence