Hydrochloric Acid → HCID 58508967, compound

Participants

Reaction Steps

Dioxane (3 mL) and a 2 mol/L aqueous solution of sodium hydroxide (1.7 mL) were added to the obtained methyl 2-(2-acetoxy-4-methylbenzamido)-4-phenylbenzoate (0.14 g), followed by stirring at room temperature for 2 hours and 30 minutes. The reaction mixture was adjusted to a pH of 3.0 with 6 mol/L hydrochloric acid. The solid substance was collected by filtration to obtain 0.042 g of 2-(2-hydroxy-4-methylbenzamido)-4-phenylbenzoic acid as a white solid.

Provenance & Evidence