Hydrochloric Acid → HCID 58508460, compound

Participants

Reaction Steps

Methanol (2 mL), dioxane (4 mL), and a 2 mol/L aqueous solution of sodium hydroxide (0.77 mL) were added to the obtained methyl 2-(2-acetoxy-3-methylbenzamido)-4-phenylbenzoate (0.062 g), followed by stirring at room temperature for 7 hours. The reaction mixture was adjusted to a pH of 1.1 with 6 mol/L hydrochloric acid. The solid substance was collected by filtration to obtain 0.044 g of 2-(2-hydroxy-3-methylbenzamido)-4-phenylbenzoic acid as a white solid.

Provenance & Evidence