HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 58508899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 58508900 | HCID 58508900 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58508899 | HCID 58508899 | — |
Reaction Steps
Ethanol (2.0 mL) and a 1 mol/L aqueous solution of sodium hydroxide (0.067 mL) were added to the obtained 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoic acid (0.032 g), followed by stirring at room temperature for 2 hours and 30 minutes. The solvent was evaporated under reduced pressure, and water was added to the obtained residue. The solid substance was collected by filtration to obtain 0.024 g of sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492582B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-05c58cbc805b4f40bfa45c7ce857e5aa |
| Source note | uspto-grants-2013_07 |