HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 46853622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 66990567 | HCID 66990567 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 46853622 | HCID 46853622 | 87.1% |
Reaction Steps
Dioxane (2 mL) and a 2 mol/L aqueous solution of sodium hydroxide (0.79 mL) were added to the obtained methyl 2-(2-acetoxy-5-(furan-2-yl)benzamido)-4-phenylbenzoate (0.072 g), followed by stirring at room temperature for 6 hours. The reaction mixture was adjusted to a pH of 1.5 with 2 mol/L hydrochloric acid, and the solid substance was collected by filtration to obtain 0.055 g of 2-(5-(furan-2-yl)-2-hydroxybenzamido)-4-phenylbenzoic acid as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492582B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-587da386385546f1a27a4d71d5d56bb7 |
| Source note | uspto-grants-2013_07 |