HRID4546

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID5820

Dibenamine

C16H18ClN

HCID11430

Potassium Carbonate

CK2O3

HCID75484

Methyl 2,3-dihydroxybenzoate

C8H8O4

PRODUCTS

生成物

结构：COC(=O)c1cccc(OCCN(Cc2ccccc2)Cc2ccccc2)c1O

HCID53929446

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

2,3-dihydroxybenzoic acid methyl ester is reacted in the presence of potassium carbonate in acetonitrile with 1.1 equivalents of 1-dibenzylamino-2-chloroethane for 18 hours at 82°. The crude 3-(2-dibenzylaminoethoxy)salicyclic acid methyl ester obtained after working up is put to further use without further purification.