1,4-Dioxane hydrochloride → HCID 66990896, compound

Participants

Reaction Steps

Ethyl acetate (1 mL) and a 4 mol/L hydrogen chloride-dioxane solution (0.50 mL) were added to the obtained tert-butyl 4-(3-hydroxy-4-(2-(methoxycarbonyl)-5-phenylphenylcarbamoyl)phenoxy)piperidine-1-carboxylate (0.025 g), followed by stirring at room temperature for 3 hours. The solid substance was collected from the reaction mixture by filtration to obtain 0.018 g of methyl 2-(2-hydroxy-4-(piperidin-4-yloxy)benzamido)-4-phenylbenzoate hydrochloride as a white solid.

Provenance & Evidence