HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → 2-(5-(2-(Diethylamino)ethoxy)-2-hydroxybenzamido)-4-phenylbenzoic acid methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 2-(5-(2-(Diethylamino)ethoxy)-2-hydroxybenzamido)-4-phenylbenzoic acid | HCID 58508815 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(5-(2-(Diethylamino)ethoxy)-2-hydroxybenzamido)-4-phenylbenzoic acid methanesulfonate | HCID 86659241 | — |
Reaction Steps
Ethanol (3.0 mL) and methanesulfonic acid (0.011 mL) were added to the obtained 2-(5-(2-(diethylamino)ethoxy)-2-hydroxybenzamido)-4-phenylbenzoic acid (0.079 g), followed by stirring at room temperature for 1 hour and 30 minutes. The solid substance was collected from the reaction mixture by filtration to obtain 0.049 g of 2-(5-(2-(diethylamino)ethoxy)-2-hydroxybenzamido)-4-phenylbenzoic acid methanesulfonate as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492582B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-6570f6aa9a7a48549a2164cf95440d39 |
| Source note | uspto-grants-2013_07 |