Methanesulfonic Acid → HCID 86659242, compound

Participants

Reaction Steps

Ethanol (2.0 mL) and methanesulfonic acid (0.010 mL) were added to the obtained 2-(2-hydroxy-4-(2-(morpholin-4-yl)ethoxy)benzamido)-4-phenylbenzoic acid (0.011 g), followed by stirring at room temperature for 3 hours and 30 minutes. The solvent was evaporated under reduced pressure, and ethanol was added to the obtained residue. The solid substance was collected by filtration to obtain 6.1 mg of 2-(2-hydroxy-4-(2-(morpholin-4-yl)ethoxy)benzamido)-4-phenylbenzoic acid methanesulfonate as a white solid.

Provenance & Evidence