HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Trifluoroacetic acid → 4-Phenyl-2-(6-phenylpyridine-3-carboxamido)benzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Trifluoroacetic acid | HCID 6422 | — |
| Edukt | Tert-butyl 4-phenyl-2-(6-phenylpyridine-3-carboxamido)benzoate | HCID 58508784 | — |
| Produkt | 4-Phenyl-2-(6-phenylpyridine-3-carboxamido)benzoic acid | HCID 58508602 | — |
Reaktionsschritte
Trifluoroacetic acid (5 mL) was added to the obtained tert-butyl 4-phenyl-2-(6-phenylpyridine-3-carboxamido)benzoate, followed by stirring at room temperature for 3 hours. The solvent was evaporated under reduced pressure, and methanol was added to the obtained residue. The solid substance was collected by filtration to obtain 53 mg of 4-phenyl-2-(6-phenylpyridine-3-carboxamido)benzoic acid as a light yellow solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08492582B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-7de150240329499c82a64376f700eb42 |
| Quellennotiz | uspto-grants-2013_07 |