HRID454732

反应详情

EQUATION

反应方程式

HRID 454732 的结构方程式

PROCEDURE

实验过程

Trifluoroacetic acid (5 mL) was added to the obtained tert-butyl 4-phenyl-2-(6-phenylpyridine-3-carboxamido)benzoate, followed by stirring at room temperature for 3 hours. The solvent was evaporated under reduced pressure, and methanol was added to the obtained residue. The solid substance was collected by filtration to obtain 53 mg of 4-phenyl-2-(6-phenylpyridine-3-carboxamido)benzoic acid as a light yellow solid.

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure, and methanol
  2. additionwas added to the obtained residue
  3. filtrationThe solid substance was collected by filtration