Methanol → HCID 66990173, compound

Participants

Reaction Steps

Methanol (5 mL), dioxane (5 mL), and a 2 mol/L aqueous solution of sodium hydroxide (0.091 mL) were added to the obtained 4-(isoquinolin-4-yl)-2-(5-phenylpyridine-3-carboxamido)benzoic acid (81 mg), and the solvent was evaporated under reduced pressure. Diisopropyl ether was added to the obtained residue, and the solid substance was collected by filtration to obtain 83 mg of sodium 4-(isoquinolin-4-yl)-2-(5-phenylpyridine-3-carboxamido)benzoate as a light yellow solid.

Provenance & Evidence