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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 454736Generated: October 30, 2026

Methanol → HCID 58508457, compound

https://huagongshe.com/reaction/454736

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 58508458HCID 58508458—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 58508457HCID 58508457—

Reaction Steps

Methanol (2 mL), dioxane (2 mL), and a 2 mol/L aqueous solution of sodium hydroxide (0.083 mL) were added to the obtained 2-(5-phenylpyridine-3-carboxamido)-4-(1H-pyrazol-1-yl)-benzoic acid (53 mg), and the solvent was evaporated under reduced pressure. Water and acetone were added to the obtained residue, and the solid substance was collected by filtration to obtain 23 mg of sodium 2-(5-phenylpyridine-3-carboxamido)-4-(1H-pyrazol-1-yl)benzoate as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08492582B2
Source datasetuspto-grants-2013_07
ORD IDord-7058e33137db454a8a9e31e807b61e12
Source noteuspto-grants-2013_07