Sodium Hydroxide → HCID 66990723, compound

Participants

Reaction Steps

Ethanol (18 mL) and a 1.0 mol/L aqueous solution of sodium hydroxide (1.3 mL) were sequentially added to the obtained 4-(2-(ethylamino)phenyl)-2-(5-phenylpyridine-3-carboxamido)benzoic acid (0.60 g), followed by stirring at room temperature for 1 hour. The solvent was evaporated under reduced pressure, and a 10% aqueous solution of ethanol was added to the obtained residue. The solid substance was collected by filtration to obtain 0.57 g of sodium 4-(2-(ethylamino)phenyl)-2-(5-phenylpyridine-3-carboxamido)benzoate as a light yellow solid.

Provenance & Evidence