HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Sodium 4-(2-fluorophenyl)-2-(5-phenylpyridine-3-carboxamido)-benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-(2-Fluorophenyl)-2-(5-phenylpyridine-3-carboxamido)benzoic acid | HCID 58508515 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Sodium 4-(2-fluorophenyl)-2-(5-phenylpyridine-3-carboxamido)-benzoate | HCID 58508514 | — |
Reaction Steps
Ethanol (1.5 mL) and a 1 mol/L aqueous solution of sodium hydroxide (0.087 mL) were sequentially added to the obtained 4-(2-fluorophenyl)-2-(5-phenylpyridine-3-carboxamido)benzoic acid (36 mg), followed by stirring at room temperature for 3 hours. The solid substance was collected by filtration to obtain 22 mg of sodium 4-(2-fluorophenyl)-2-(5-phenylpyridine-3-carboxamido)-benzoate as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492582B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-9f892ce130fd41d28e01b5164eb52546 |
| Source note | uspto-grants-2013_07 |