Sodium Hydroxide → HCID 58508811, compound

Participants

Reaction Steps

A 1 mol/L aqueous solution of sodium hydroxide (0.10 mL) was added to an ethanol (4.0 mL) suspension of the obtained 2-(5-phenylpyridine-3-carboxamido)-4-(thiophen-3-yl)benzoic acid (47 mg) at room temperature, followed by stirring at the same temperature for 1 hour and 10 minutes. The solvent was evaporated under reduced pressure, and ethanol and water were added to the obtained residue. The solid substance was collected by filtration to obtain 40 mg of sodium 2-(5-phenylpyridine-3-carboxamido)-4-(thiophen-3-yl)benzoate as a white solid.

Provenance & Evidence