HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 58508715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 58508716 | HCID 58508716 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58508715 | HCID 58508715 | — |
Reaction Steps
Dioxane (2 mL), methanol (2 mL), and a 2 mol/L aqueous solution of sodium hydroxide (0.025 mL) were added to the obtained 4-phenyl-2-(6-(pyridin-4-yl)pyridine-3-carboxamido)benzoic acid (20 mg), and the solvent was evaporated under reduced pressure. Acetone was added to the obtained residue. The solid substance was collected by filtration to obtain 17 mg of sodium 4-phenyl-2-(6-(pyridin-4-yl)pyridine-3-carboxamido)benzoate as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08492582B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-b0bf01f1ce2949f0a9ebd60641c1bf5b |
| Source note | uspto-grants-2013_07 |