HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 86646560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3,6-Dichloropyridazine | HCID 67331 | — |
| Reactant | 3-Fluoro-1-propanol | HCID 68042 | — |
| Product | HCID 86646560 | HCID 86646560 | 87% |
Reaction Steps
3-(3-Fluoropropoxy)-6-chloropyridazine (108c, 557 mg, 87%) was prepared in the same manner as in Example 26 as a white solid using sodium hydride (NaH 60%, 202 mg, 5.04 mmol), 3,6-dichloropyridazine (107, 500 mg, 3.36 mmol) and 3-fluoro-1-propanol (393 mg, 5.04 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497260B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-c817411a81be4171adfddef722521826 |
| Source note | uspto-grants-2013_07 |