1-Methylpiperazine → HCID 178480642, compound

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Reaction Steps

The title compound was prepared following the procedure described for 6a using 1-methylpiperazine instead of piperazine. 1H-NMR (DMSO-d6) δ (ppm): 2.52 (3H, s), 2.84 (4H, brm), 3.62 (4H, brm), 7.11 (1H, t, J=7.22 Hz), 7.20 (1H, d, J=9.28 Hz), 7.40 (2H, dd, J=8.30, 7.57 Hz), 7.80 (1H, d, J=9.28 Hz), 8.21 (2H, d, J=7.57 Hz), 8.50 (1H, s). m/z 361.4 (MH+).

Provenance & Evidence