HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 67029007, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 2-(6-Methyl-2-p-tolyl-imidazo[1,2-a]pyridin-3-ylmethyl)-2H-[1,2,4]triazole-3-carboxylic acid methylamide | HCID 67027485 | — |
| Reactant | HCID 67028732 | HCID 67028732 | — |
| Product | HCID 67029007 | HCID 67029007 | — |
Reaction Steps
The title compound was prepared according to the procedure described for compound 68 from methyl 1-((2-(4-chlorophenyl)imidazo[1,2-a]pyridin-3-yl)methyl)-1H-1,2,4-triazole-5-carboxylate and dimethylamine. 1H-NMR (400 MHz, CDCl3, δ) 8.21 (d, J=6.9 Hz, 1H), 7.97 (s, 1H), 7.71 (d, J=9.2 Hz, 1H), 7.68 (d, J=8.5 Hz, 2H), 7.49 (d, J=8.4 Hz, 1H), 7.34 (m, 1H), 6.94 (m, 1H), 5.80 (s, 2H), 3.21 (s, 3H), 3.13 (s, 3H) ppm; m/e 241, 243.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497278B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-d16f7ba6a50c49d9b3c81a244d120b4d |
| Source note | uspto-grants-2013_07 |