反应详情

The title compound was prepared according to the procedure described for compound 68 from methyl 1-((2-(4-chlorophenyl)imidazo[1,2-b]pyridazin-3-yl)methyl)-1H-1,2,4-triazole-5-carboxylate and methylamine. 1H-NMR (CDCl3, 400 MHz, δ) 8.42 (dd, J=1.5, 4.4 Hz, 1H), 8.31 (s, 1H), 8.04 (dd, J=1.5, 9.2 Hz, 1H), 7.95 (d, J=8.5 Hz, 2H), 7.52 (d, J=8.5 Hz, 2H), 7.20 (dd, J=4.5, 9.2 Hz, 1H), 7.06 (broad, 1H), 5.91 (s, 2H), 3.00 (d, J=5.1 Hz, 3H)ppm; m/e 368 (M+H)+.