Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 455076Generated: October 31, 2026

Dimethylamine → HCID 67028507, compound

https://huagongshe.com/reaction/455076

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamineHCID 674—
ReactantHCID 58337018HCID 58337018—
ReactantHCID 67028967HCID 67028967—
ProductHCID 67028507HCID 67028507—

Reaction Steps

The title compound was prepared according to the experimental for compound 132 from 4-chloro-1-((2-(4-chlorophenyl)imidazo[1,2-a]pyridin-3-yl)methyl)pyrimidin-2(1H)-one and dimethylamine. M/e+ 380 for C20H19ClN5O (M+H)+; 1H-NMR (400 MHz, CDCl3) δ 8.44 (d, J=6.9 Hz, 1H), 7.67 (d, J=8.4 Hz, 2H), 7.63 (d, J=8.8 Hz, 1H), 7.47 (d, J=8.4 Hz, 2H), 7.28 (d, J=6.9 Hz, 1H), 6.86 (t, J=6.6 Hz, 1H), 6.75 (d, J=7.7 Hz, 1H), 5.63 (d, J=7.7 Hz, 1H), 5.56 (s, 2H), 3.18 (s, 3H), 2.96 (s, 3H) ppm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08497278B2
Source datasetuspto-grants-2013_07
ORD IDord-e12396d8643940278023f179e9c78dc6
Source noteuspto-grants-2013_07