HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-azido-N-methylbutane-1-sulfonamide → HCID 61456555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-azido-N-methylbutane-1-sulfonamide | HCID 71699855 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 61456555 | HCID 61456555 | — |
Reaction Steps
To a solution of 4-azido-N-methylbutane-1-sulfonamide (Example 6; 202 mmol), in methanol (200 ml) was added Pd/C (20 mmol Pd). The mixture put under an hydrogen atmosphere and was stirred overnight at r.t. The mixture was filtered and concentrated. The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497270B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-156ee17ba7614877b82ac41c0a9b55e4 |
| Source note | uspto-grants-2013_07 |