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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 455294Generated: October 29, 2026

4-azido-N-methylbutane-1-sulfonamide → HCID 61456555, compound

https://huagongshe.com/reaction/455294

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-azido-N-methylbutane-1-sulfonamideHCID 71699855—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 61456555HCID 61456555—

Reaction Steps

To a solution of 4-azido-N-methylbutane-1-sulfonamide (Example 6; 202 mmol), in methanol (200 ml) was added Pd/C (20 mmol Pd). The mixture put under an hydrogen atmosphere and was stirred overnight at r.t. The mixture was filtered and concentrated. The crude product was used in the next step without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08497270B2
Source datasetuspto-grants-2013_07
ORD IDord-156ee17ba7614877b82ac41c0a9b55e4
Source noteuspto-grants-2013_07