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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 455301Generated: October 29, 2026

Potassium Carbonate → HCID 67109896, compound

https://huagongshe.com/reaction/455301

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 67109671HCID 67109671—
ReactantHCID 86667510HCID 86667510—
SolventDimethylformamideHCID 6228—
ProductHCID 67109896HCID 67109896—

Reaction Conditions

Temperature80 °C

Reaction Steps

A mixture of tert-butyl 4-fluoro-2-hydroxybenzylcarbamate (Example 15; 12.2 mmol), 4-iodo-N-methylbutane-1-sulfonamide (Example 18; 18.3 mmol) and potassium carbonate (61 mmol) in DMF (60 ml) was stirred at 80° C. for 10 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08497270B2
Source datasetuspto-grants-2013_07
ORD IDord-f61a1fcee0f144cb9800243ce325e5fc
Source noteuspto-grants-2013_07