HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 455301Generated: October 29, 2026
Potassium Carbonate → HCID 67109896, compound
https://huagongshe.com/reaction/455301
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 67109671 | HCID 67109671 | — |
| Reactant | HCID 86667510 | HCID 86667510 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67109896 | HCID 67109896 | — |
Reaction Steps
A mixture of tert-butyl 4-fluoro-2-hydroxybenzylcarbamate (Example 15; 12.2 mmol), 4-iodo-N-methylbutane-1-sulfonamide (Example 18; 18.3 mmol) and potassium carbonate (61 mmol) in DMF (60 ml) was stirred at 80° C. for 10 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08497270B2 |
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| Source dataset | uspto-grants-2013_07 |
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| ORD ID | ord-f61a1fcee0f144cb9800243ce325e5fc |
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| Source note | uspto-grants-2013_07 |
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