HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → HCID 50915826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | HCID 59341976 | HCID 59341976 | — |
| Reactant | 1-(Quinolin-6-ylmethyl)-1H-[1,2,3]triazolo[4,5-b]pyrazine-6-carbohydrazonamide | HCID 66927091 | — |
| Product | HCID 50915826 | HCID 50915826 | — |
Reaction Steps
The title compound was prepared in analogy to the synthesis of compound 64.2 from 1-(quinolin-6-ylmethyl)-1H-[1,2,3]triazolo[4,5-b]pyrazine-6-carbonitrile and hydrazinecarbox-amide hydrochloride. 1H-NMR (400 MHz, DMSO-d6) δ ppm 9.80 (s, 1H), 8.88 (m, 1H), 8.34 (d, 1H), 8.05 (d, 1H), 8.00 (d, 1H), 7.86 (d, 1H), 7.52 (dd, 1H), 6.18 (s, 2H). LCMS (method B): [MH]+=363, tR=1.70 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497368B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-18922038128c41c5a9e63dbb0b9fb41b |
| Source note | uspto-grants-2013_07 |