HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68019351, compound → HCID 70197892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68019351 | HCID 68019351 | — |
| Solvent | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 70197892 | HCID 70197892 | — |
Reaction Steps
A solution of tert-butyl (2-{[(3R,4R)-1-benzyl-4-{(3-methylbutyl)[(4-nitrophenyl)sulfonyl]amino}pyrrolidin-3-yl]amino}ethyl)carbamate in 2N HCl dioxane was stirred overnight at room temperature before the solvent was evaporated to dryness. The resulting tris HCl salt was used directly in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497383B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-3c544afde81045bcbe2fb4527f148a07 |
| Source note | uspto-grants-2013_07 |