HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70198456, compound → HCID 67776146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70198456 | HCID 70198456 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67776146 | HCID 67776146 | — |
Reaction Steps
Benzyl (3S*,4R*)-1-(tert-butoxycarbonyl)-4-(3-hydroxypropyl)pyrrolidin-3-ylcarbamate (0.98 g, 2.59 mmol) was hydrogenated over 10% Pd/C (0.05 g) in MeOH for 3 hours at ambient pressure. The catalyst was filtered off and the solvent was evaporated giving the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497383B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-d9d71ce723994eaaacad3c184a3e7052 |
| Source note | uspto-grants-2013_07 |