HRID456343

反应详情

EQUATION

反应方程式

HRID 456343 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of (1R,2S)-2-aminocyclopentanecarboxylic acid (0.15 g, 0.9 mmol) in methanol (5 mL) was added 4N HCl in dioxane (1 mL) and the reaction mixture was stirred at reflux overnight. The reaction mixture was concentrated in vacuo to afford an oil which was used directly for the next step.

WORKUP

后处理

  1. temperatureat reflux overnight
  2. concentrationThe reaction mixture was concentrated in vacuo
  3. customto afford an oil which