HCID 69420852, compound → HCID 69423162, compound

Participants

Reaction Steps

4-[2-(2-Benzyloxycarbonylamino-propoxy)-phenyl]-piperazine-1-carboxylic acid tert-butyl ester (5.7 g, 12.15 mmol) and 10% wet palladium on carbon (5.0 g) were dissolved in methanol (200 mL) at r.t. The solution was stirred under hydrogen for about 4 hours. The mixture was filtered through a bed of celite. The solvent was removed under reduced pressure to afford the title compound as a colorless oil (4.2 g, 100%).

Provenance & Evidence