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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 456624Generated: October 29, 2026

Hydrazine hydrate (1:1) → HCID 178478094, compound

https://huagongshe.com/reaction/456624

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
ReactantHCID 18436870HCID 18436870—
SolventEthanolHCID 702—
ProductHCID 178478094HCID 178478094—

Reaction Steps

A mixture of (2-chloro-pyridin-3-yl)-[3-(2,6-dichloro-phenyl)-1H-pyrrol-2-yl]-methanone (160 mg) and hydrazine hydrate (0.5 mL) in ethanol (8 mL) was heated at 90–100° C. for 24 hours. The reaction was concentrated, the residue was purified on a silica gel column to give 30 mg of the titled compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07186716B2
Source datasetuspto-grants-2007_03
ORD IDord-c2c7d35a9480407bb22f5496e0259f3d
Source noteuspto-grants-2007_03