HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178478094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 18436870 | HCID 18436870 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178478094 | HCID 178478094 | — |
Reaction Steps
A mixture of (2-chloro-pyridin-3-yl)-[3-(2,6-dichloro-phenyl)-1H-pyrrol-2-yl]-methanone (160 mg) and hydrazine hydrate (0.5 mL) in ethanol (8 mL) was heated at 90–100° C. for 24 hours. The reaction was concentrated, the residue was purified on a silica gel column to give 30 mg of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07186716B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-c2c7d35a9480407bb22f5496e0259f3d |
| Source note | uspto-grants-2007_03 |