HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 456629Generated: October 29, 2026
Hydrazine hydrate (1:1) → HCID 178477869, compound
https://huagongshe.com/reaction/456629
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | (2,6-dichloro-pyridin-3-yl)-(1H-pyrrol-3-yl)-methanone | HCID 18436868 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178477869 | HCID 178477869 | — |
Reaction Steps
A mixture of (2,6-dichloro-pyridin-3-yl)-(1H-pyrrol-3-yl)-methanone (300 mg) and hydrazine hydrate (0.2 mL) in ethanol (10 mL) was heated at 90° C. for 20 hours. The reaction was concentrated to 6 mL, diluted with water (2 mL) and cooled. The precipitate was collected and dried to give 160 mg of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07186716B2 |
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| Source dataset | uspto-grants-2007_03 |
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| ORD ID | ord-e8c5a7615b094a128dc5606ce408285f |
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| Source note | uspto-grants-2007_03 |
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