HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 135432876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pyridine-4-carbonyl chloride | HCID 417436 | — |
| Reactant | HCID 136358049 | HCID 136358049 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 135432876 | HCID 135432876 | 104.1% |
Reaction Steps
2,2-Dimethyl-propionic acid 5-amino-3-(1H-pyrrol-2-yl)-indazol-1-yl ester (0.38 mmol) was coupled with isonicotinoyl chloride (0.4 mmol) (Aldrich, Milwaukee, Wis.) and triethylamine in DCM at 0° C. to give 120 mg of the titled compound as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07186716B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-cd59e749b76049bf95308e179f83d795 |
| Source note | uspto-grants-2007_03 |