HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 456679Generated: October 26, 2026
Hydrazine hydrate (1:1) → HCID 178527317, compound
https://huagongshe.com/reaction/456679
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | (1-benzenesulfonyl-1H-pyrrol-2-yl)-(2-chloro-pyridin-3-yl)-methanone | HCID 18436866 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178527317 | HCID 178527317 | — |
Reaction Steps
A mixture of (1-benzenesulfonyl-1H-pyrrol-2-yl)-(2-chloro-pyridin-3-yl)-methanone (150 mg) and hydrazine hydrate (0.15 mL) in ethanol (3.5 mL) was heated at 90° C. for overnight. The reaction was concentrated, diluted with ethyl acetate, washed with base and water, dried and concentrated to give 75 mg of the titled compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07186716B2 |
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| Source dataset | uspto-grants-2007_03 |
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| ORD ID | ord-5d87d57c9bb84d86bdd354d24a7bbeee |
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| Source note | uspto-grants-2007_03 |
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