HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl oxoacetate → HCID 178472742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl oxoacetate | HCID 70211 | — |
| Reactant | 1-Phenethylamine, (-)- | HCID 75818 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178472742 | HCID 178472742 | — |
Reaction Steps
To a (1S)-1-phenylethanamine (77.4 mL), was added a solution of ethyl glyoxylate in toluene (45–50%, 123 mL) at room temperature. After 1 hr, the mixture was evaporated in vacuo. The residue (120 g) was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07186731B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-80f9469bc3c646f8a01f1776fe8e0bb4 |
| Source note | uspto-grants-2007_03 |